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The compounds were then milled for 2 min using a two-roll mill (Polymix-110L; Servitec Maschinenservice in Wustermark, Germany) at 50 C with a friction ratio of 1:1.2. Densities for the raw materials were used to determine values of filler volume fraction (φ), which was nearly constant at 0.15 to 0.17 for the four compounds ( Table 1 ).

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